2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

Base Information

Chemical Name:2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate
CAS No.:1428847-53-3
Molecular Formula:C₂₃H₂₇NO₉S
Molecular Weight:493.535
Hs Code.:

Synonyms:2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

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Chemical Property of 2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

Chemical Property:

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Technology Process of 2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

There total 6 articles about 2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1428847-52-2
3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoic acid

: 30379-58-9
benzyl glycolate

: 1428847-53-3
2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 24812-90-6
methyl 3-amino-4-methoxybenzoate

: 1428847-53-3
2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 2 h / 20 °C

2: dmap / dichloromethane / 2 h / 20 °C

3: tin(II) chloride dihdyrate; lithium hydroxide / tetrahydrofuran / 24 h / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C

With pyridine; dmap; tin(II) chloride dihdyrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 29655-68-3
methyl 4-methoxy-3-(methylsulfonamido)benzoate

: 1428847-53-3
2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / 2 h / 20 °C

2: tin(II) chloride dihdyrate; lithium hydroxide / tetrahydrofuran / 24 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C

With dmap; tin(II) chloride dihdyrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane;