6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

Base Information

Chemical Name:6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine
CAS No.:1332625-71-4
Molecular Formula:C₃₂H₃₀N₂O₂
Molecular Weight:474.602
Hs Code.:

Synonyms:6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

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Chemical Property of 6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

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Technology Process of 6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

There total 3 articles about 6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1332625-70-3
6-bromo-6′-(2-methoxy-5-methylphenyl)-2,2′-bipyridine

: 104115-76-6
3-methoxynaphthalen-2-ylboronic acid

: 1332625-71-4
6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; water; toluene; at 80 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c1dt10124b

Reference yield:

: 49669-22-9
6,6'-Dibromo-2,2'-bipyridine

: 1332625-71-4
6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 60 h / 75 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 20 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; water; toluene; 1: Suzuki-Miyaura reaction / 2: Suzuki-Miyaura reaction;
DOI:10.1039/c1dt10124b

Reference yield:

: 128733-85-7
(5-(tert-butyl)-2-methoxyphenyl)boronic acid

: 1332625-71-4
6-(5-tert-butyl-2-methoxyphenyl)-6'-(3-methoxynaphthalen-2-yl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 60 h / 75 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 20 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; water; toluene; 1: Suzuki-Miyaura reaction / 2: Suzuki-Miyaura reaction;
DOI:10.1039/c1dt10124b