benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

Base Information

Chemical Name:benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester
CAS No.:884864-17-9
Molecular Formula:C₁₈H₂₅BO₄
Molecular Weight:316.205
Hs Code.:

Synonyms:benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

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Technology Process of benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

There total 2 articles about benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100330-28-7
pent-4-yn-1-yl benzoate

: 73183-34-3
bis(pinacol)diborane

: 884864-17-9
benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

Guidance literature:: With water; In toluene; at 80 ℃; for 10h; regioselective reaction; Schlenk technique; Sealed tube;
DOI:10.1021/jacs.1c08088

Reference yield: 72.0%

: 100330-28-7
pent-4-yn-1-yl benzoate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 884864-17-9
benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

Guidance literature:: With bis(cyclohexanyl)borane; at 20 ℃; for 16h;
DOI:10.1021/ol0601850

Reference yield: 44.0%

: 884864-17-9
benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester

: 3240-34-4
[bis(acetoxy)iodo]benzene

: (E)-5-benzoyloxypent-1-enyl(phenyl)iodonium tetrafluoroborate

Guidance literature:: benzoic acid (E)-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pent-4-enyl ester; [bis(acetoxy)iodo]benzene; With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at 0 ℃; for 1.5h;

With sodium tetrafluoroborate; In dichloromethane; water; at 0 ℃;
DOI:10.1021/ol0601850