4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

Base Information

Chemical Name:4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester
CAS No.:1343456-51-8
Molecular Formula:C₁₇H₁₆BrNO₃
Molecular Weight:362.223
Hs Code.:

Synonyms:4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

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Chemical Property of 4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

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Technology Process of 4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

There total 1 articles about 4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 94-09-7
p-aminoethylbenzoate

: 262450-65-7
3-bromo-5-methoxybenzaldehyde

: 1343456-51-8
4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

Guidance literature:: In ethanol; for 2h; Reflux;

Reference yield: 100.0%

: 1343456-51-8
4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

: 78-84-2
isobutyraldehyde

: 1343456-53-0
2-(3-bromo-5-methoxy-phenyl)-4-hydroxy-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester

Guidance literature:: With water; ytterbium(III) trifluoromethanesulfonate hydrate; In tetrahydrofuran; at 25 ℃; for 5h;

Reference yield:

: 1343456-51-8
4-{[1-(3-bromo-5-methoxy-phenyl)-methylidene]-amino}-benzoic acid ethyl ester

: 1343456-50-7
2-(3-Methoxy-5-morpholin-4-yl-phenyl)-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: water / ytterbium(III) trifluoromethanesulfonate hydrate / tetrahydrofuran / 5 h / 25 °C

2: trifluoroacetic acid; triethylsilane / 1 h / 25 °C

3: potassium carbonate / copper(l) iodide; N,N-dimethylglycine hydrochoride / dimethyl sulfoxide / 4 h / 120 °C

4: water; lithium hydroxide monohydrate / tetrahydrofuran; methanol / 12 h / 60 °C

With triethylsilane; lithium hydroxide monohydrate; water; potassium carbonate; trifluoroacetic acid; copper(l) iodide; ytterbium(III) trifluoromethanesulfonate hydrate; N,N-dimethylglycine hydrochoride; In tetrahydrofuran; methanol; dimethyl sulfoxide; 1: Diels-Alder Reaction / 3: Ullmann Reaction;