N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

Base Information

Chemical Name:N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide
CAS No.:1579281-60-9
Molecular Formula:C₁₆H₁₆BrFN₂O₄S
Molecular Weight:431.282
Hs Code.:

Synonyms:N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

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Chemical Property of N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

Chemical Property:

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Technology Process of N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

There total 4 articles about N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 349-88-2
4-Fluorobenzenesulfonyl chloride

: C₁₀H₁₃BrN₂O₂

: 1579281-60-9
N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2014.01.053

Reference yield:

: 1579281-56-3
N,N-dimethyl-5-bromo-2-methoxy-3-nitrobenzamide

: 1579281-60-9
N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; tin(II) chloride dihdyrate / water / 20 °C

2: pyridine / 0 - 20 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; In water;
DOI:10.1016/j.ejmech.2014.01.053

Reference yield:

: C₈H₅BrClNO₄

: 1579281-60-9
N,N-dimethyl-5-bromo-2-methoxy-3-(4-fluorophenylsulfonamino)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.5 h / 20 °C / Cooling with ice

2: hydrogenchloride; tin(II) chloride dihdyrate / water / 20 °C

3: pyridine / 0 - 20 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; In tetrahydrofuran; water;
DOI:10.1016/j.ejmech.2014.01.053