iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

Base Information

Chemical Name:iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone
CAS No.:107112-67-4
Molecular Formula:C₂₁H₃₅N₂O₂*I
Molecular Weight:474.426
Hs Code.:

Synonyms:iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

Chemical Property:

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Technology Process of iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

There total 5 articles about iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107112-64-1,107112-65-2
N,N-dimethylhydrazone de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

: 74-88-4
methyl iodide

: 107112-67-4
iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

Guidance literature:: for 24h;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 107112-67-4
iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / p-toluene sulfonic acid / CH₂Cl₂

2: 1.4 M n-butyllithium / tetrahydrofuran; hexane

3: 100 percent / 24 h

With n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 41302-05-0
1-chloro-4-tetrahydropyranyloxybutane

: 107112-67-4
iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 (tetrahydropyrannyle ether)-6 hexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.4 M n-butyllithium / tetrahydrofuran; hexane

2: 100 percent / 24 h

With n-butyllithium; In tetrahydrofuran; hexane;