N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

Base Information

Chemical Name:N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide
CAS No.:1179329-83-9
Molecular Formula:C₂₄H₂₅F₅N₄O₆S
Molecular Weight:592.544
Hs Code.:

N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

Synonyms:N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

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Chemical Property of N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

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Technology Process of N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

There total 7 articles about N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006899-36-0
1-(2-amino-4-fluorobenzyl)-3-(4-fluoro-3-trifluoromethyl-phenyl)-5,5-dimethylimidazolidine-2,4-dione

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 1179329-83-9
N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 76437-44-0
1-(bromomethyl)-4-fluoro-2-nitrobenzene

: 1179329-83-9
N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile

2: H3B*NMe3 / 20 % Pd(OH)2/C / methanol / 4 h / Reflux; Inert atmosphere

3: triethylamine / dichloromethane / 20 °C

With H₃B*NMe₃; caesium carbonate; triethylamine; 20 % Pd(OH)2/C; In methanol; dichloromethane; acetonitrile;

Reference yield:

: 1179329-78-2
1-(4-fluoro-2-nitrobenzyl)-3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethylimidazolidine-2,4-dione

: 1179329-83-9
N-{5-fluoro-2-[3-(4-fluoro-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}N'-tert-butyloxycarbonylsulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: H3B*NMe3 / 20 % Pd(OH)2/C / methanol / 4 h / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 20 °C

With H₃B*NMe₃; triethylamine; 20 % Pd(OH)2/C; In methanol; dichloromethane;