C₁₂H₁₅BrN₂O₂

Base Information

Chemical Name:C₁₂H₁₅BrN₂O₂
CAS No.:1354455-85-8
Molecular Formula:C₁₂H₁₅BrN₂O₂
Molecular Weight:299.167
Hs Code.:

C<sub>12</sub>H<sub>15</sub>BrN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₅BrN₂O₂

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Chemical Property of C₁₂H₁₅BrN₂O₂

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Technology Process of C₁₂H₁₅BrN₂O₂

There total 1 articles about C₁₂H₁₅BrN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3282-30-2
pivaloyl chloride

: 112253-70-0
2-amino-4-bromobenzamide

: 1354455-85-8
C₁₂H₁₅BrN₂O₂

Guidance literature:: 2-amino-4-bromobenzamide; With triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

pivaloyl chloride; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1354455-85-8
C₁₂H₁₅BrN₂O₂

: 1354455-88-1
N-[4-(2-tert-butyl-4-chloroquinazolin-7-yl)phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 1.5 h / Inert atmosphere; Reflux

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 115 °C / Inert atmosphere; Microwave irradiation; Sealed tube

3: N,N-diethylaniline; trichlorophosphate / benzene / 6 h / Reflux

With sodium carbonate; N,N-diethylaniline; sodium hydroxide; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; ethanol; water; toluene; benzene; 2: Suzuki Coupling;

Reference yield:

: 1354455-85-8
C₁₂H₁₅BrN₂O₂

: 1354455-89-2
C₂₆H₂₈N₄O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol; water / 1.5 h / Inert atmosphere; Reflux

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 115 °C / Inert atmosphere; Microwave irradiation; Sealed tube

3: N,N-diethylaniline; trichlorophosphate / benzene / 6 h / Reflux

4: caesium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 1 h / Inert atmosphere; Sealed tube; Heating

With sodium carbonate; caesium carbonate; N,N-diethylaniline; sodium hydroxide; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; ethanol; water; toluene; benzene; 2: Suzuki Coupling / 4: Suzuki Coupling;