7-decyl-3,2',3',5',6'-pentamethoxyflavone

Base Information

Chemical Name:7-decyl-3,2',3',5',6'-pentamethoxyflavone
CAS No.:1354708-28-3
Molecular Formula:C₃₀H₄₀O₇
Molecular Weight:512.643
Hs Code.:

Synonyms:7-decyl-3,2',3',5',6'-pentamethoxyflavone

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Chemical Property of 7-decyl-3,2',3',5',6'-pentamethoxyflavone

Chemical Property:

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Technology Process of 7-decyl-3,2',3',5',6'-pentamethoxyflavone

There total 7 articles about 7-decyl-3,2',3',5',6'-pentamethoxyflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1354708-22-7
1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',3'',5'',6''-tetramethoxyphenyl)propane-1,3-dione

: 1354708-28-3
7-decyl-3,2',3',5',6'-pentamethoxyflavone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1139/v11-087

Reference yield:

: 2441-46-5
1,2,4,5-tetramethoxybenzene

: 1354708-28-3
7-decyl-3,2',3',5',6'-pentamethoxyflavone

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / Inert atmosphere

1.2: Inert atmosphere

2.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water; dimethyl sulfoxide / Inert atmosphere

3.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 1.08 h / -78 - 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With sodium chlorite; n-butyllithium; thionyl chloride; trimethylsilyl trifluoromethanesulfonate; aminosulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1139/v11-087

Reference yield:

: 30225-87-7
2,4,5-trimethoxyphenyl formate

: 1354708-28-3
7-decyl-3,2',3',5',6'-pentamethoxyflavone

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; potassium hydroxide / tetrahydrofuran / Inert atmosphere

2.1: potassium hydroxide / tetrahydrofuran; water / Inert atmosphere

3.1: n-butyllithium / Inert atmosphere

3.2: Inert atmosphere

4.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water; dimethyl sulfoxide / Inert atmosphere

5.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 1.08 h / -78 - 20 °C / Inert atmosphere

6.3: 20 °C / Inert atmosphere

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With sodium chlorite; n-butyllithium; thionyl chloride; trimethylsilyl trifluoromethanesulfonate; aminosulfonic acid; water; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1139/v11-087