o-FC₆H₄C≡CAg

Base Information

• Chemical Name: o-FC₆H₄C≡CAg
• CAS No.: 1190964-59-0
• Molecular Formula: C₈H₄AgF
• Molecular Weight: 226.986

Synonyms:o-FC₆H₄C≡CAg

Chemical Property of o-FC₆H₄C≡CAg

Chemical Property:

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Technology Process of o-FC₆H₄C≡CAg

There total 1 articles about o-FC₆H₄C≡CAg which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

(2-fluorophenyl)acetylene (766-49-4) + silver nitrate → o-FC6H4C≡CAg (1190964-59-0)

Guidance literature:

With Et₃N; In acetonitrile; ligand and Et3N in MeCN mixed with MeCN soln. of Ag compd. (1:1 molar ratio), stirred for 10 h; ppt. filtered off, washed (MeCN, H2O), stored at -10°C;

DOI:10.1016/j.poly.2009.05.004

Reference yield: 44.0%

o-FC6H4C≡CAg (1190964-59-0) + silver nitrate → 5NO3(1-)*10C8H4F(1-)*Ag15(15+)

Guidance literature:

In dimethyl sulfoxide;

DOI:10.1021/om5003733

Reference yield:

silver tetrafluoroborate (14104-20-2) + hexafluoroglutaric acid (376-73-8) + o-FC6H4C≡CAg (1190964-59-0) + acetonitrile (75-05-8,26809-02-9) + silver(l) oxide (20667-12-3) → [silver(I) 2-fluorophenylethynide]*Ag2(hexafluoroglutarate)*2MeCN

Guidance literature:

In water; acetonitrile; AgBF4 (2 mmol), Ag2O (0.5 mmol), and ligand (0.5 mmol) dissolved in H2O/MeCN mixt., Ag compd. added, stirred for 4 h; filtered, crystd. on storage at room temp. in dark for 2 wk, elem. anal.;

DOI:10.1016/j.poly.2009.05.004

upstream raw materials:

(2-fluorophenyl)acetylene

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