meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

Base Information

Chemical Name:meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin
CAS No.:80447-62-7
Molecular Formula:C₆₇H₇₀N₈O₅S
Molecular Weight:1099.41
Hs Code.:

meso-β-<o-<6-(acetylthio)hexanamido>phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

Synonyms:meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

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Chemical Property of meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

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Technology Process of meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

There total 4 articles about meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 80441-39-0
meso-β--α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

: 507-09-5
tiolacetic acid

: 80447-62-7
meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

Guidance literature:: With potassium carbonate; In acetone; for 12h;
DOI:10.1021/ja00369a041

Reference yield:

: 502-44-3,24980-41-4,80137-66-2
hexahydro-2H-oxepin-2-one

: 80447-62-7
meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / conc. HBr, conc. H₂SO₄ / 10 h / Heating

2: 98 percent / thionyl chloride / 1.) room temperature, 1 h, 2.) reflux

3: 70 percent / pyridine / CH₂Cl₂ / 12 h

4: 67 percent / potassium carbonate / acetone / 12 h

With pyridine; thionyl chloride; sulfuric acid; hydrogen bromide; potassium carbonate; In dichloromethane; acetone;
DOI:10.1021/ja00369a041

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 80447-62-7
meso-β-phenyl>-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / thionyl chloride / 1.) room temperature, 1 h, 2.) reflux

2: 70 percent / pyridine / CH₂Cl₂ / 12 h

3: 67 percent / potassium carbonate / acetone / 12 h

With pyridine; thionyl chloride; potassium carbonate; In dichloromethane; acetone;
DOI:10.1021/ja00369a041