cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

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Chemical Name:cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate
CAS No.:1207109-01-0
Molecular Formula:C₅₉H₈₃N₃O₈S₂
Molecular Weight:1026.46
Hs Code.:

cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

Synonyms:cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

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Chemical Property of cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

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Technology Process of cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

There total 3 articles about cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207108-98-2
cholest-5-en-3-yl (2R)-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-3-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}propanoate

: 1207109-01-0
cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / dichloromethane / 0.33 h / 20 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 0 °C / Inert atmosphere

3: dimethyl sulfoxide / 2 h / 20 °C

With piperidine; triethylsilane; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1248/cpb.59.1386

Reference yield:

: 57-88-5
cholesterol

: 1207109-01-0
cholest-5-en-3-yl (13R)-13-amino-1-(2-naphthyl)-6-oxo-2-(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)-5,7-dioxa-10,11-dithia-2-azatetradecan-14-oate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h / 20 °C

2: piperidine / dichloromethane / 0.33 h / 20 °C

3: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 0 °C / Inert atmosphere

4: dimethyl sulfoxide / 2 h / 20 °C

With piperidine; triethylsilane; dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1248/cpb.59.1386