1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

Base Information

Chemical Name:1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime
CAS No.:154458-58-9
Molecular Formula:C₁₇H₂₉NO₃Si
Molecular Weight:323.508
Hs Code.:

Synonyms:1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

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Chemical Property of 1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

Chemical Property:

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Technology Process of 1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

There total 5 articles about 1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 67-62-9
O-Methylhydroxylamin

: 154458-57-8
1-benzyloxy-3-(tert-butyldimethylsilyloxy)propan-2-one

: 154458-58-9
1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

Guidance literature:: In ethanol;
DOI:10.1016/S0040-4039(00)61686-6

Reference yield:

: 13071-59-5,17325-85-8,56552-80-8,4799-67-1
3-benzyloxypropan-1,2-diol

: 154458-58-9
1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / imidazole / dimethylformamide / Ambient temperature

2: 80 percent / pyridinium chlorochromate / CH₂Cl₂ / 72 h / 45 °C

3: 66 percent / ethanol

With 1H-imidazole; pyridinium chlorochromate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)61686-6

Reference yield:

: 100-39-0
benzyl bromide

: 154458-58-9
1-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-propan-2-one O-methyl-oxime

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NaH, Et₄NI / tetrahydrofuran / Ambient temperature

2: 98 percent / HCl / tetrahydrofuran / Ambient temperature

3: 82 percent / imidazole / dimethylformamide / Ambient temperature

4: 80 percent / pyridinium chlorochromate / CH₂Cl₂ / 72 h / 45 °C

5: 66 percent / ethanol

With 1H-imidazole; hydrogenchloride; tetraethylammonium iodide; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)61686-6