2-methoxy benzyl propynoate

Base Information

• Chemical Name: 2-methoxy benzyl propynoate
• CAS No.: 131530-53-5
• Molecular Formula: C₁₁H₁₀O₃
• Molecular Weight: 190.199

Synonyms:2-methoxy benzyl propynoate

Chemical Property of 2-methoxy benzyl propynoate

Chemical Property:

Purity/Quality:

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Technology Process of 2-methoxy benzyl propynoate

There total 2 articles about 2-methoxy benzyl propynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

dicyclohexyl-carbodiimide (538-75-0) + Propiolic acid (471-25-0) → N-cyclohexyl-N-(cyclohexylcarbamoyl)propiolamide (40886-85-9) + 2-methoxy benzyl propynoate (131530-53-5)

Guidance literature:

With dmap; (2-methoxyphenyl)methanol; In diethyl ether; for 10h; Ambient temperature;

Reference yield: 15.0%

(2-methoxyphenyl)methanol (612-16-8) + Propiolic acid (471-25-0) → N-cyclohexyl-N-(cyclohexylcarbamoyl)propiolamide (40886-85-9) + 2-methoxy benzyl propynoate (131530-53-5)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In diethyl ether; for 10h; Ambient temperature;

Reference yield: 38.5%

methylthiol (74-93-1) + 2-methoxy benzyl propynoate (131530-53-5) → (Z)-3-Methylsulfanyl-acrylic acid 2-methoxy-benzyl ester (131530-54-6) + isotachin 'C' (107584-57-6)

Guidance literature:

With triethylamine; In diethyl ether; at 0 ℃; for 24h; Yield given;

upstream raw materials:

dicyclohexyl-carbodiimide

Propiolic acid

(2-methoxyphenyl)methanol

Downstream raw materials:

(Z)-3-Methylsulfanyl-acrylic acid 2-methoxy-benzyl ester

isotachin 'C'

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