(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

Base Information

Chemical Name:(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH
CAS No.:1400743-57-8
Molecular Formula:C₃₅H₄₄N₄O₇
Molecular Weight:632.757
Hs Code.:

Synonyms:(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

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Chemical Property of (benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

Chemical Property:

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Technology Process of (benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

There total 4 articles about (benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 623-04-1
4-aminobenzenemethanol

: 114480-07-8
(S)-2-((S)-2-(((benzyloxy)carbonyl)amino)-3-phenylpropanamido)-6-((tert-butoxycarbonyl)amino)hexanoic acid

: 1400743-57-8
(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1021/jm500544p

Reference yield:

: C₃₃H₄₅N₃O₉

: 623-04-1
4-aminobenzenemethanol

: 1400743-57-8
(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

Guidance literature:: In tetrahydrofuran; at -15 - 20 ℃; Inert atmosphere;
DOI:10.1039/b919329d

Reference yield:

: 2418-95-3
(S)-2-amino-6-(tert-butoxycarbonylamino)hexanoic acid

: 1400743-57-8
(benzyloxycarbonyl)-Phe-Lys-N-ε-(tert-butoxycarbonyl)-(p-aminobenzyl)-OH

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 20 °C

2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; water;
DOI:10.1021/jm500544p