C₂₃H₂₃N₃O₃

Base Information

Chemical Name:C₂₃H₂₃N₃O₃
CAS No.:1363373-89-0
Molecular Formula:C₂₃H₂₃N₃O₃
Molecular Weight:389.454
Hs Code.:

C<sub>23</sub>H<sub>23</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₃N₃O₃

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Chemical Property of C₂₃H₂₃N₃O₃

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Technology Process of C₂₃H₂₃N₃O₃

There total 11 articles about C₂₃H₂₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1363373-88-9
C₂₈H₃₁N₃O₅

: 1363373-89-0
C₂₃H₂₃N₃O₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 14h; Inert atmosphere;

Reference yield:

: 75867-41-3
4-trimethylsilanylethynyl-benzoic acid methyl ester

: 1363373-89-0
C₂₃H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; methanol / 3 h / 20 °C / Inert atmosphere

2.1: pyridine / copper diacetate / methanol / 48 h / 20 °C / Inert atmosphere

3.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

3.2: pH 2

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; copper diacetate; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 619-44-3
methyl 4-iodobenzoate

: 1363373-89-0
C₂₃H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 22 h / 60 °C / Inert atmosphere; Sealed vessel

2.1: potassium carbonate; methanol / 3 h / 20 °C / Inert atmosphere

3.1: pyridine / copper diacetate / methanol / 48 h / 20 °C / Inert atmosphere

4.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

4.2: pH 2

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;