(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

Base Information Edit

Chemical Name:(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate
CAS No.:1093192-04-1
Molecular Formula:C₁₄H₂₀N₂O₄
Molecular Weight:280.324
Hs Code.:
Mol file:1093192-04-1.mol

Synonyms:(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

Suppliers and Price of (S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate Edit

Chemical Property:

Boiling Point:393.6±42.0 °C(Predicted)
Density:1.132±0.06 g/cm3(Predicted)

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

There total 2 articles about (S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1093192-03-0
(S)-3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoic acid

: 74-88-4
methyl iodide

: 1093192-04-1
(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

Guidance literature:: (S)-3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoic acid; With caesium carbonate; In N,N-dimethyl-formamide; for 0.166667h; Sonication for 1 min;

methyl iodide; In N,N-dimethyl-formamide; at 10 - 20 ℃; for 2.41667h;

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1093192-04-1
(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water / 45 °C / Inert atmosphere

1.2: 3 h / 35 - 46 °C / Inert atmosphere

1.3: 12 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

2.2: 13.25 h / 0 - 20 °C / Inert atmosphere

2.3: pH 7 - 8

With caesium carbonate; potassium hydroxide; In water; N,N-dimethyl-formamide;