C₂₁H₂₈O₂S₃

Base Information

Chemical Name:C₂₁H₂₈O₂S₃
CAS No.:90344-13-1
Molecular Formula:C₂₁H₂₈O₂S₃
Molecular Weight:408.65
Hs Code.:

C<sub>21</sub>H<sub>28</sub>O<sub>2</sub>S<sub>3</sub>

Synonyms:C₂₁H₂₈O₂S₃

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Chemical Property of C₂₁H₂₈O₂S₃

Chemical Property:

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Technology Process of C₂₁H₂₈O₂S₃

There total 15 articles about C₂₁H₂₈O₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 109-80-8
1.3-propanedithiol

: 90367-63-8
(4aS,7R,8R,8aR)-8-Benzenesulfonylmethyl-7-methyl-3,4,4a,7,8,8a-hexahydro-2H-naphthalen-1-one

: 90344-13-1
C₂₁H₂₈O₂S₃

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 15h;
DOI:10.1021/ja00325a017

Reference yield:

: 80106-30-5
(4E,6E)-octa-4,6-dien-1-ol

: 90344-13-1
C₂₁H₂₈O₂S₃

Guidance literature:: Multi-step reaction with 13 steps

1: 95 percent / pyridine / 15 h / 5 °C

2: 94 percent / NaOMe / methanol / 2 h

3: 75 percent / 40 percent peracetic acid / ethyl acetate / 2 h / -20 - 0 °C

4: 70 percent / benzene / 24 h / 80 °C

5: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

7: aluminum amalgam / tetrahydrofuran; H₂O / 3 h

8: 92 percent / NaOMe / methanol / 24 h / 40 °C

9: 100 percent / TsOH / benzene / 72 h / 80 °C / Dean-Stark apparatus

10: 91 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

11: Me₃SiCl, NaI / acetonitrile / 1 h

12: benzene / 3 h / 80 °C / dark

13: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h

With pyridine; peracetic acid; lithium aluminium tetrahydride; chloro-trimethyl-silane; aluminium amalgam; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00325a017

Reference yield:

: 68823-50-7
methyl (4E,6E)-octa-4,6-dienoate

: 90344-13-1
C₂₁H₂₈O₂S₃

Guidance literature:: Multi-step reaction with 14 steps

1: 99 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

2: 95 percent / pyridine / 15 h / 5 °C

3: 94 percent / NaOMe / methanol / 2 h

4: 75 percent / 40 percent peracetic acid / ethyl acetate / 2 h / -20 - 0 °C

5: 70 percent / benzene / 24 h / 80 °C

6: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

8: aluminum amalgam / tetrahydrofuran; H₂O / 3 h

9: 92 percent / NaOMe / methanol / 24 h / 40 °C

10: 100 percent / TsOH / benzene / 72 h / 80 °C / Dean-Stark apparatus

11: 91 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

12: Me₃SiCl, NaI / acetonitrile / 1 h

13: benzene / 3 h / 80 °C / dark

14: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h

With pyridine; peracetic acid; lithium aluminium tetrahydride; chloro-trimethyl-silane; aluminium amalgam; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00325a017