thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

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Chemical Name:thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester
CAS No.:1207681-56-8
Molecular Formula:C₂₉H₃₁N₃O₅S
Molecular Weight:533.648
Hs Code.:

Synonyms:thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

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Chemical Property of thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

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Technology Process of thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

There total 6 articles about thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207681-54-6
(R)-4-benzyl-3-((R)-3-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-phenyl}-2-thiocyanato-propionyl)-oxazolidin-2-one

: 1207681-56-8
thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

Guidance literature:: With water; platinum tris(dimethylphosphine oxide); In tetrahydrofuran; at 40 ℃; for 2h; Inert atmosphere;

Reference yield:

: 5223-06-3
5-ethyl-2-(2-hydroxyethyl)pyridine

: 1207681-56-8
thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate / toluene / 113 h / 20 °C / Reflux; Inert atmosphere

3.1: water; lithium hydroxide monohydrate / 1,4-dioxane / Inert atmosphere

3.2: pH 6 - 7 / Inert atmosphere

4.1: triethylamine; pivaloyl chloride / toluene / 22.5 h / 80 °C / Reflux; Inert atmosphere

5.1: lithium diisopropyl amide / tetrahydrofuran; hexanes / 0.5 h / -78 °C / Inert atmosphere

5.2: 1.83 h / -78 °C / Inert atmosphere

6.1: water / platinum tris(dimethylphosphine oxide) / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; pivaloyl chloride; potassium carbonate; triethylamine; lithium diisopropyl amide; platinum tris(dimethylphosphine oxide); In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; toluene;

Reference yield:

: 1207681-51-3
3-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-phenyl}-propionic acid methyl ester

: 1207681-56-8
thiocarbamic acid S-((R)-2-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-1-{4-[2-(5-ethyl-pyridin-2-yl)-ethoxy]-benzyl}-2-oxo-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; lithium hydroxide monohydrate / 1,4-dioxane / Inert atmosphere

1.2: pH 6 - 7 / Inert atmosphere

2.1: triethylamine; pivaloyl chloride / toluene / 22.5 h / 80 °C / Reflux; Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexanes / 0.5 h / -78 °C / Inert atmosphere

3.2: 1.83 h / -78 °C / Inert atmosphere

4.1: water / platinum tris(dimethylphosphine oxide) / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; pivaloyl chloride; triethylamine; lithium diisopropyl amide; platinum tris(dimethylphosphine oxide); In tetrahydrofuran; 1,4-dioxane; hexanes; toluene;