2,6-Dichloroisonicotinamide

Base Information

Chemical Name:2,6-Dichloroisonicotinamide
CAS No.:89281-13-0
Molecular Formula:C6H4Cl2N2O
Molecular Weight:191.017
Hs Code.:2933399090
European Community (EC) Number:674-279-8
DSSTox Substance ID:DTXSID00381861
Wikidata:Q72466588
Mol file:89281-13-0.mol

Synonyms:2,6-Dichloroisonicotinamide;89281-13-0;2,6-dichloropyridine-4-carboxamide;2,6-Dichloro-4-pyridinecarboxamide;MFCD00052640;Oprea1_674830;SCHEMBL3281481;DTXSID00381861;CFYBBFGXTQBLQV-UHFFFAOYSA-N;AKOS009077364;PS-4483;SB52351;2,6-dichloroisonicotinamide, AldrichCPR;AC-14633;SY032124;CS-0151393;FT-0610615;D86224;A843108

Suppliers and Price of 2,6-Dichloroisonicotinamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,6-Dichloroisonicotinamide
1g
$ 145.00

TRC
2,6-Dichloroisonicotinamide
500mg
$ 105.00

TRC
2,6-Dichloroisonicotinamide
250mg
$ 65.00

SynQuest Laboratories
2,6-Dichloroisonicotinamide
1 g
$ 32.00

Oakwood
2,6-Dichloroisonicotinamide 90%
5g
$ 152.00

Oakwood
2,6-Dichloroisonicotinamide 90%
250mg
$ 22.00

Oakwood
2,6-Dichloroisonicotinamide 90%
1g
$ 43.00

Matrix Scientific
2,6-Dichloroisonicotinamide
500mg
$ 30.00

Matrix Scientific
2,6-Dichloroisonicotinamide
1g
$ 44.00

Matrix Scientific
2,6-Dichloroisonicotinamide
5g
$ 153.00

Total 28 raw suppliers

Chemical Property of 2,6-Dichloroisonicotinamide

Chemical Property:

Vapor Pressure:0.00129mmHg at 25°C
Melting Point:202 °C
Refractive Index:1.603
Boiling Point:298.1 °C at 760 mmHg
Flash Point:134.1 °C
PSA：55.98000
Density:1.524 g/cm³
LogP:2.18760
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:0.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:189.9700681
Heavy Atom Count:11
Complexity:155

Purity/Quality:

99%, ^*data from raw suppliers

2,6-Dichloroisonicotinamide ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(N=C1Cl)Cl)C(=O)N

Technology Process of 2,6-Dichloroisonicotinamide

There total 9 articles about 2,6-Dichloroisonicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 98027-84-0
2,6-dichloro-4-iodopyridine

: 3019-71-4
Trichloroacetyl isocyanate

: 89281-13-0
2,6-dichloropyridine-4-carboxamide

Guidance literature:: 2,6-dichloro-4-iodopyridine; With chloro-trimethyl-silane; ethylene dibromide; lithium chloride; zinc; In tetrahydrofuran; at 18 ℃; Inert atmosphere;

Trichloroacetyl isocyanate; In tetrahydrofuran; at -20 - 25 ℃; Inert atmosphere;

With methanol; potassium carbonate; In tetrahydrofuran; at 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol101469f

Reference yield:

: 5398-44-7
2,6-dichloropyridine-4-carboxylic acid

: 89281-13-0
2,6-dichloropyridine-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

With thionyl chloride;

Reference yield:

: 2402-78-0
2,6-dichloropyridine

: 64-18-6
formic acid

: 89281-13-0
2,6-dichloropyridine-4-carboxamide

Guidance literature:: 2,6-dichloropyridine; formic acid; With ruthenium-carbon composite; trifluoroacetic anhydride; In dimethyl sulfoxide; at 5 - 90 ℃; for 0.833333h; Inert atmosphere;

With ammonia; In dimethyl sulfoxide; at 140 ℃; for 2h; under 750.075 Torr;