3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine

Base Information

• Chemical Name: 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine
• CAS No.: 1363774-60-0
• Molecular Formula: C₃₃H₄₈N₄O₉Si₂
• Molecular Weight: 700.937

Synonyms:3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine

Chemical Property of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine

Chemical Property:

Purity/Quality:

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Technology Process of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine

There total 3 articles about 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O₆-benzylinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

succinic acid anhydride (108-30-5) + 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O6-benzylinosine (1363774-58-6) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O6-benzylinosine (1363774-60-0)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1080/15257770.2011.650254

Reference yield:

sodium phenyl-methanolate (20194-18-7) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O6-benzylinosine (1363774-60-0)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; benzyl alcohol / 5 h / 20 °C / Inert atmosphere

2: pyridine / 4 h / 20 °C / Inert atmosphere

3: pyridine; dmap / 6 h / 20 °C / Inert atmosphere

With pyridine; dmap; In N,N-dimethyl-formamide; benzyl alcohol;

DOI:10.1080/15257770.2011.650254

Reference yield:

O6-benzylinosine (42204-35-3) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-succinyl-O6-benzylinosine (1363774-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 4 h / 20 °C / Inert atmosphere

2: pyridine; dmap / 6 h / 20 °C / Inert atmosphere

With pyridine; dmap;

DOI:10.1080/15257770.2011.650254

upstream raw materials:

succinic acid anhydride

3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O₆-benzylinosine

O⁶-benzylinosine

sodium phenyl-methanolate

Downstream raw materials:

2'-O-succinyl-O₆-benzylinosine

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