4-chloro-N-(2-bromophenyl)benzothioamide

Base Information

Chemical Name:4-chloro-N-(2-bromophenyl)benzothioamide
CAS No.:459128-66-6
Molecular Formula:C₁₃H₉BrClNS
Molecular Weight:326.644
Hs Code.:

Synonyms:4-chloro-N-(2-bromophenyl)benzothioamide

Suppliers and Price of 4-chloro-N-(2-bromophenyl)benzothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(2-bromophenyl)benzothioamide

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Technology Process of 4-chloro-N-(2-bromophenyl)benzothioamide

There total 2 articles about 4-chloro-N-(2-bromophenyl)benzothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-36-1
2-bromoaniline

: 459128-66-6
4-chloro-N-(2-bromophenyl)benzothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 24 h / 20 °C

2: Lawessons reagent / toluene / 4 h / Reflux

With Lawessons reagent; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2019.151082

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 459128-66-6
4-chloro-N-(2-bromophenyl)benzothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 24 h / 20 °C

2: Lawessons reagent / toluene / 4 h / Reflux

With Lawessons reagent; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2019.151082

Reference yield: 97.0%

: 459128-66-6
4-chloro-N-(2-bromophenyl)benzothioamide

: 6265-91-4
2-(4-chlorophenyl)benzothiazole

Guidance literature:: With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 3h;
DOI:10.1039/c6ra18510j