N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

Base Information

Chemical Name:N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside
CAS No.:1198155-85-9
Molecular Formula:C₃₈H₄₆N₄O₉
Molecular Weight:702.805
Hs Code.:

Synonyms:N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

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Chemical Property of N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

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Technology Process of N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

There total 1 articles about N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1198156-13-6
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-3-O-benzyl-2-deoxy-α-D-glycopyranoside

: 123-76-2
levulinic acid

: 1198155-85-9
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

Guidance literature:: N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-3-O-benzyl-2-deoxy-α-D-glycopyranoside; levulinic acid; With 2-chloro-1-methyl-pyridinium iodide; In dichloromethane; at 20 ℃; for 0.25h;

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/ja907358k

Reference yield: 95.0%

: ethyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α/β-L-idopyranoside

: 1198155-85-9
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

: 1198156-99-8
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-(2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-α-L-idopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: ethyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α/β-L-idopyranoside; N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;
DOI:10.1021/ja907358k

Reference yield: 92.0%

: 889129-00-4
(2R,4aR,6S,7R,8S,8aR)-8-(benzyloxy)-6-(ethylthio)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-7-yl 4-oxopentanoate

: 1198155-85-9
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside

: 1198156-91-0
N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-(2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: (2R,4aR,6S,7R,8S,8aR)-8-(benzyloxy)-6-(ethylthio)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-7-yl 4-oxopentanoate; N-(benzyl)-benzyloxycarbonyl-5-aminopentyl O-2-azido-6-O-levulinoyl-3-O-benzyl-2-deoxy-α-D-glycopyranoside; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;
DOI:10.1021/ja907358k