D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

Base Information

Chemical Name:D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol
CAS No.:847555-66-2
Molecular Formula:C₁₆H₂₃Cl₃FNO₆
Molecular Weight:450.719
Hs Code.:

Synonyms:D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

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Technology Process of D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

There total 2 articles about D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 125290-99-5
(1S,2S,3R,4S,5S,6S)-1-fluoro-2-O-(methyl)cyclohexane-2,3,4,5,6-pentol

: 75-87-6
chloral

: 538-75-0
dicyclohexyl-carbodiimide

: 847555-66-2
D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

Guidance literature:: In 1,2-dichloro-ethane; for 6h; Heating;
DOI:10.1016/j.tetlet.2004.11.158

Reference yield:

: 642-38-6
quebrachitol

: 847555-66-2
D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: diethylaminosulfur trifluoride / CH₂Cl₂ / 4 h / 20 °C

2: 61 percent / 1,2-dichloro-ethane / 6 h / Heating

With diethylamino-sulfur trifluoride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2004.11.158

Reference yield: 40.0%

: 108-24-7
acetic anhydride

: 847555-66-2
D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol

: 847673-10-3
D-1,3,4,5,6-penta-O-acetyl-2-deoxy-2-fluoro-chiro-inositol

Guidance literature:: D-1-O-cyclohexylcarbamoyl-2-deoxy-2-fluoro-3-O-methyl-5,6-O-[(R/S)-2,2,2-trichloroethylidene]-chiro-inositol; With hydrogen; nickel; In ethanol; at 20 ℃; for 8h;

With hydrogen iodide; In water; for 2h; Heating;

acetic anhydride; With pyridine; at 20 ℃; for 12h;
DOI:10.1016/j.carres.2004.11.031