N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

Base Information

Chemical Name:N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine
CAS No.:153108-98-6
Molecular Formula:C₂₁H₃₅NO₃Si
Molecular Weight:377.599
Hs Code.:

Synonyms:N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

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Chemical Property of N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

Chemical Property:

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Technology Process of N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

There total 6 articles about N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 39945-50-1
2-(2-hydroxyethyl)-piperidine-1-carboxylic acid benzyl ester

: 153108-98-6
N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

Reference yield:

: 1484-84-0
2(RS)-(2-hydroxyethyl)piperidine

: 18162-48-6
tert-butyldimethylsilyl chloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 153108-98-6
N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

Guidance literature:: 2(RS)-(2-hydroxyethyl)piperidine; benzyl chloroformate; With sodium carbonate; In water; acetone;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In N,N-dimethyl-formamide;

Reference yield:

: 1484-84-0
2(RS)-(2-hydroxyethyl)piperidine

: 153108-98-6
N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 20percent aq. Na₂CO₃ / CH₂Cl₂ / 1 h / Ambient temperature

2: 99 percent / imidazole, 4-(dimethylamino)pyridine / dimethylformamide / 0.5 h / Ambient temperature

With 1H-imidazole; dmap; sodium carbonate; In dichloromethane; N,N-dimethyl-formamide;