[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

Base Information

Chemical Name:[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride
CAS No.:214141-78-3
Molecular Formula:C₂₅H₂₃BiF₅NO₂
Molecular Weight:673.436
Hs Code.:

Synonyms:[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

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Chemical Property of [2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

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Technology Process of [2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

There total 4 articles about [2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: xenon fluoride

: 214141-82-9
[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuthane

: 214141-78-3
[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

Guidance literature:: In dichloromethane; acetonitrile; Ar-atmosphere; XeF2 addn. (1 equiv.) at -20°C, warming to room temp. with stirring (2 h); evapn. (vac.), crystn. (CH2Cl2/hexane 1/10); elem. anal.;
DOI:10.1021/om990597v

Reference yield:

: 33397-21-6
tris(4-methoxyphenyl)bismuth

: 214141-78-3
[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium; triflic acid; HMPA / tetrahydrofuran; dichloromethane; methanol

2: magnesium; triflic acid; HMPA / tetrahydrofuran; dichloromethane; methanol

3: acetonitrile; dichloromethane

With magnesium; triflic acid; HMPA; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/om990597v

Reference yield:

: 32664-13-4
2-(2-bromo-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

: 214141-78-3
[2-(4,4-dimethyl-3,4-dihydrooxaol-2-yl)phenyl](4-methoxyphenyl)(4-trifluoromethylphenyl)bismuth difluoride

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium; triflic acid; HMPA / tetrahydrofuran; dichloromethane; methanol

2: magnesium; triflic acid; HMPA / tetrahydrofuran; dichloromethane; methanol

3: acetonitrile; dichloromethane

With magnesium; triflic acid; HMPA; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/om990597v