C₃₄H₆₄O₄S₂Si₂

Base Information

Chemical Name:C₃₄H₆₄O₄S₂Si₂
CAS No.:1513700-71-4
Molecular Formula:C₃₄H₆₄O₄S₂Si₂
Molecular Weight:657.183
Hs Code.:

C<sub>34</sub>H<sub>64</sub>O<sub>4</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₃₄H₆₄O₄S₂Si₂

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Chemical Property of C₃₄H₆₄O₄S₂Si₂

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Technology Process of C₃₄H₆₄O₄S₂Si₂

There total 12 articles about C₃₄H₆₄O₄S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1513700-61-2
C₂₂H₄₈O₂S₂Si₂

: 1513700-69-0
C₁₂H₁₇IO₂

: 1513700-71-4
C₃₄H₆₄O₄S₂Si₂

Guidance literature:: C₂₂H₄₈O₂S₂Si₂; With tert.-butyl lithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.25h; Inert atmosphere;

C₁₂H₁₇IO₂; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.75h; Inert atmosphere;
DOI:10.1021/ol403423r

Reference yield:

: 1513700-49-6
C₂₃H₃₇NO₅Si

: 1513700-71-4
C₃₄H₆₄O₄S₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: trimethylaluminum / dichloromethane; toluene / 1.5 h / 0 - 20 °C / Inert atmosphere

1.2: 3 h / -20 - 20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / -78 - 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

4.1: magnesium bromide ethyl etherate / diethyl ether / 16 h / 0 - 20 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.25 h / -78 °C / Inert atmosphere

5.2: 0.75 h / Inert atmosphere

With 2,6-dimethylpyridine; trimethylaluminum; tert.-butyl lithium; diisobutylaluminium hydride; magnesium bromide ethyl etherate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol403423r

Reference yield:

: 1513700-52-1
C₁₅H₃₃NO₄Si

: 1513700-71-4
C₃₄H₆₄O₄S₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,6-dimethylpyridine / dichloromethane / -78 - 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

3.1: magnesium bromide ethyl etherate / diethyl ether / 16 h / 0 - 20 °C / Inert atmosphere

4.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.25 h / -78 °C / Inert atmosphere

4.2: 0.75 h / Inert atmosphere

With 2,6-dimethylpyridine; tert.-butyl lithium; diisobutylaluminium hydride; magnesium bromide ethyl etherate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1021/ol403423r