methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate

Base Information

• Chemical Name: methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate
• CAS No.: 221554-79-6
• Molecular Formula: C₂₈H₂₉Cl₃N₂O₅
• Molecular Weight: 579.908

Synonyms:methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate

Chemical Property of methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate

Chemical Property:

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Technology Process of methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate

There total 3 articles about methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate (172405-21-9) + 2,2,2-Trichloroethyl chloroformate (17341-93-4) → methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate (221554-79-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1016/S0040-4020(98)01211-3

Reference yield:

mono-4-methoxytrityl chloride (14470-28-1) → methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate (221554-79-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 1 h / -40 - -25 °C

2: 97 percent / triethylamine / CH₂Cl₂ / 0 °C

With triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

N-(2-aminoethyl)glycine methyl ester hydrochloride → methyl N-<2-(N-Mmt)aminoethyl>-N-glycinate (221554-79-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 1 h / -40 - -25 °C

2: 97 percent / triethylamine / CH₂Cl₂ / 0 °C

With triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(02)00527-6

upstream raw materials:

methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

2,2,2-Trichloroethyl chloroformate

mono-4-methoxytrityl chloride

Downstream raw materials:

[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetic acid

C₅₀H₆₀Cl₆N₈O₁₄

C₅₁H₆₂Cl₆N₈O₁₄

[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

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