(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4

Base Information

• Chemical Name: (CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4
• CAS No.: 162588-66-1
• Molecular Formula: C₁₃H₃₄N₃PRh*C₃₂H₁₂BF₂₄
• Molecular Weight: 1229.53

Synonyms:(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4

Chemical Property of (CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4

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Technology Process of (CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4

There total 1 articles about (CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]B(C₆H₃(CF₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(CH2)6N3(CH3)3RhP(CH3)3(CH3)H(1+)*SO3CF3(1-)=[(CH2)6N3(CH3)3RhP(CH3)3(CH3)H]SO3CF3 (162588-69-4) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → (CH2)6N3(CH3)3RhP(CH3)3(CH3)H(1+)*B(C6H3(CF3)2)4(1-)=[(CH2)6N3(CH3)3RhP(CH3)3(CH3)H]B(C6H3(CF3)2)4 (162588-66-1)

Guidance literature:

In chlorobenzene; elem. anal.;

DOI:10.1021/ja00110a025

Reference yield:

(CH2)6N3(CH3)3RhP(CH3)3(CH3)H(1+)*B(C6H3(CF3)2)4(1-)=[(CH2)6N3(CH3)3RhP(CH3)3(CH3)H]B(C6H3(CF3)2)4 (162588-66-1) + benzene-d6 (1076-43-3) → (CH2)6N3(CH3)3RhP(CH3)3(C6(2)H5)(2)H(1+)*B(C6H3(CF3)2)4(1-)=[(CH2)6N3(CH3)3RhP(CH3)3(C6(2)H5)(2)H]B(C6H3(CF3)2)4

Guidance literature:

In benzene-d6; 75°C;

DOI:10.1021/ja00110a025

Reference yield:

(CH2)6N3(CH3)3RhP(CH3)3(CH3)H(1+)*B(C6H3(CF3)2)4(1-)=[(CH2)6N3(CH3)3RhP(CH3)3(CH3)H]B(C6H3(CF3)2)4 (162588-66-1) + methane (6532-48-5) → (CH2)6N3(CH3)3RhP(CH3)3((13)CH3)H(1+)*B(C6H3(CF3)2)4(1-)=[(CH2)6N3(CH3)3RhP(CH3)3((13)CH3)H]B(C6H3(CF3)2)4 (162615-56-7)

Guidance literature:

In further solvent(s); 80°C, pressure of methane 18 atm.;

DOI:10.1021/ja00110a025

upstream raw materials:

(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H⁽¹⁺⁾*SO₃CF₃^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(CH₃)H]SO₃CF₃

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

Downstream raw materials:

(CH₂)6N₃(CH₃)3RhP(CH₃)3(⁽¹³⁾CH₃)H⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(CH₂)6N₃(CH₃)3RhP(CH₃)3(⁽¹³⁾CH₃)H]B(C₆H₃(CF₃)2)4

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