11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Base Information

Chemical Name:11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one
CAS No.:312626-58-7
Molecular Formula:C₂₆H₂₄N₂O₂
Molecular Weight:396.489
Hs Code.:
DSSTox Substance ID:DTXSID801124528

Synonyms:11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one;CBMicro_038897;Cambridge id 5957532;Oprea1_234618;DTXSID801124528;CCG-16685;STK067081;AKOS001617175;BIM-0038743.P001;EU-0038368;SR-01000434228;SR-01000434228-1;2,3,4,5,10,11-Hexahydro-11-(4-methoxyphenyl)-3-phenyl-1H-dibenzo[b,e][1,4]diazepin-1-one;312626-58-7

Suppliers and Price of 11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:396.183778013
Heavy Atom Count:30
Complexity:645

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2C3=C(CC(CC3=O)C4=CC=CC=C4)NC5=CC=CC=C5N2

Technology Process of 11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

There total 4 articles about 11-(4-methoxyphenyl)-3-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 3-(2-aminophenylamino)-5-phenylcyclohex-2-enone

: 123-11-5
4-methoxy-benzaldehyde

: 312626-58-7
3-phenyl-11-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: With acetic acid; In ethanol; Reflux;
DOI:10.3184/174751914X14138073011066

Reference yield:

: 100-52-7
benzaldehyde

: 312626-58-7
3-phenyl-11-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide

2: sodium ethanolate

3: toluene / 8 h / Reflux

4: acetic acid / ethanol / Reflux

With sodium ethanolate; acetic acid; sodium hydroxide; In ethanol; toluene;
DOI:10.3184/174751914X14138073011066

Reference yield:

: 493-72-1
5-phenyl-cyclohexane-1,3-dione

: 312626-58-7
3-phenyl-11-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 8 h / Reflux

2: acetic acid / ethanol / Reflux

With acetic acid; In ethanol; toluene;
DOI:10.3184/174751914X14138073011066