1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate

Base Information

• Chemical Name: 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate
• CAS No.: 129086-10-8
• Molecular Formula: C₂₄H₃₄O₈S
• Molecular Weight: 482.595

Synonyms:1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate

Chemical Property of 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate

There total 6 articles about 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(2-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}ethoxy)ethanol (57671-28-0,1201808-31-2) + p-toluenesulfonyl chloride (98-59-9) → 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate (129086-10-8)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1016/j.tetlet.2019.151475

Reference yield:

Pentaethylene glycol (4792-15-8) → 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate (129086-10-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 12 h / Ambient temperature

2: pyridine / 0 °C

With pyridine; sodium hydride; In tetrahydrofuran;

DOI:10.1021/ja00091a005

Reference yield:

benzyl bromide (100-39-0) → 1-phenyl-2,5,8,11,14-pentaoxahexadecan-16-yl 4-methylbenzene-1-sulfonate (129086-10-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 12 h / Ambient temperature

2: pyridine / 0 °C

With pyridine; sodium hydride; In tetrahydrofuran;

DOI:10.1021/ja00091a005

upstream raw materials:

2-(2-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}ethoxy)ethanol

p-toluenesulfonyl chloride

triethylene glycol monobenzyl ether

2-[2-(2-{2-[2-(2-benzyloxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

Downstream raw materials:

{2-[2-(2-{2-[2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octyloxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxymethyl}-benzene

{2-[2-(2-{2-[2-(2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-heptyloxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxymethyl}-benzene

[2-(2-{2-[2-(2-Azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxymethyl]-benzene

2-(2-{2-[2-(2-Benzyloxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethylamine

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