4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

Base Information

Chemical Name:4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol
CAS No.:459430-98-9
Molecular Formula:C₂₈H₂₅FO₄S
Molecular Weight:476.569
Hs Code.:

Synonyms:4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

Chemical Property:

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Technology Process of 4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

There total 11 articles about 4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 459430-97-8
(4-{4-(Benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)(triisopropyl)silane

: 459430-98-9
4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

Guidance literature:: With tetrabutyl ammonium fluoride; In 1,1-dichloroethane; ethyl acetate;

Reference yield:

: 459430-91-2
{[4-(benzyloxy)-3-bromobenzyl]oxy}(tert-butyl)dimethylsilane

: 459430-98-9
4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

Guidance literature:: Multi-step reaction with 7 steps

1: ammonium chloride; tert.-butyl lithium / tetrahydrofuran; hexane

2: dichloromethane; ethyl acetate

3: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran; ethyl acetate

4: dichloromethane

5: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

6: triethylsilane; ammonium chloride / tetrahydrofuran

7: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-n-butylammoniumfluoride trihydrate; In tetrahydrofuran; 1,1-dichloroethane; hexane; dichloromethane; ethyl acetate;

Reference yield:

: 459430-95-6
4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzaldehyde

: 459430-98-9
4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

2: triethylsilane; ammonium chloride / tetrahydrofuran

3: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1,1-dichloroethane; hexane; ethyl acetate;