Technology Process of 4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol
There total 11 articles about 4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
1,1-dichloroethane; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: ammonium chloride; tert.-butyl lithium / tetrahydrofuran; hexane
2: dichloromethane; ethyl acetate
3: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran; ethyl acetate
4: dichloromethane
5: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane
6: triethylsilane; ammonium chloride / tetrahydrofuran
7: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate
With
triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-n-butylammoniumfluoride trihydrate;
In
tetrahydrofuran; 1,1-dichloroethane; hexane; dichloromethane; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane
2: triethylsilane; ammonium chloride / tetrahydrofuran
3: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate
With
triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; 1,1-dichloroethane; hexane; ethyl acetate;