5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

Base Information

Chemical Name:5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)
CAS No.:322732-68-3
Molecular Formula:C₅₀H₄₅Cl₂N₂O₉P
Molecular Weight:919.795
Hs Code.:

Synonyms:5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

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Chemical Property of 5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

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Technology Process of 5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

There total 1 articles about 5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1883-32-5
2,2-diphenyl ethanol

: 53676-18-9
2,5-dichlorophenyl phosphorodichloridate

: 42926-80-7
5'-O-(4-monomethoxytrityl)-2'-deoxythymidine

: 322732-68-3
5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

Guidance literature:: 2,5-dichlorophenyl phosphorodichloridate; With 1,2,4-Triazole; In pyridine; at 0 ℃; for 0.5h;

5'-O-(4-monomethoxytrityl)-2'-deoxythymidine; In pyridine; for 1h;

2,2-diphenyl ethanol; In pyridine; for 24h;
DOI:10.1002/1522-2675(20001108)83:11<3053::AID-HLCA3053>3.0.CO;2-X

Reference yield: 79.0%

: 121-44-8
triethylamine

: 322732-68-3
5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate)

: 5'-O-(monomethoxytrityl)thymidine 3'-[2,2-diphenylethyl triethylammonium phosphate]

Guidance literature:: triethylamine; With 4-nitrobenzaldehyde oxime; In 1,4-dioxane; water; at 20 ℃; for 0.166667h;

5'-O-(monomethoxytrityl)thymidine 3'-(2,5-dichlorophenyl 2,2-diphenylethyl phosphate); In 1,4-dioxane; water; for 2.5h;
DOI:10.1002/1522-2675(20001108)83:11<3053::AID-HLCA3053>3.0.CO;2-X