t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

Base Information

Chemical Name:t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate
CAS No.:1333379-28-4
Molecular Formula:C₂₂H₂₇NO₆S
Molecular Weight:433.525
Hs Code.:

Synonyms:t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

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Chemical Property of t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

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Technology Process of t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

There total 7 articles about t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1333379-27-3
t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 1333379-28-4
t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

Guidance literature:: t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate; With methanol; potassium hydroxide; for 4h; Reflux;

epichlorohydrin; In formic acid; at 20 ℃; for 0.25h;

Reference yield:

: 1333379-26-2
S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

: 1333379-28-4
t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: iron; ammonium chloride / methanol; water / 2 h / Inert atmosphere; Reflux

2: triethylamine / methanol / 24 h / 20 °C / Inert atmosphere

3: potassium hydroxide / methanol / 4 h / Inert atmosphere; Reflux

4: methanol / 20 °C / Inert atmosphere

With iron; ammonium chloride; triethylamine; potassium hydroxide; In methanol; water;
DOI:10.1021/jm200566e

Reference yield:

: 350672-95-6
4-fluoro-2-(methoxymethoxy)-1-nitrobenzene

: 1333379-28-4
t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2: iron; ammonium chloride / methanol; water / 2 h / Inert atmosphere; Reflux

3: triethylamine / methanol / 24 h / 20 °C / Inert atmosphere

4: potassium hydroxide / methanol / 4 h / Inert atmosphere; Reflux

5: methanol / 20 °C / Inert atmosphere

With iron; ammonium chloride; caesium carbonate; triethylamine; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm200566e