t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

Base Information

Chemical Name:t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate
CAS No.:1333379-30-8
Molecular Formula:C₂₂H₂₇NO₇S₂
Molecular Weight:481.591
Hs Code.:

Synonyms:t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

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Chemical Property of t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

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Technology Process of t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

There total 9 articles about t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1333379-29-5
t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)-carbamate

: 1333379-30-8
t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

Guidance literature:: With thiourea; In methanol; dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm200566e

Reference yield:

: 1333379-28-4
t-butyl (2-(methoxymethoxy)-4-(4-((oxiran-2-ylmethyl)thio)phenoxy)phenyl)-carbamate

: 1333379-30-8
t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 - 2 °C / Inert atmosphere

2: thiourea / methanol; dichloromethane / 24 h / 20 °C / Inert atmosphere

With thiourea; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/jm200566e

Reference yield:

: 1333379-26-2
S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

: 1333379-30-8
t-butyl (2-(methoxymethoxy)-4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: iron; ammonium chloride / methanol; water / 2 h / Inert atmosphere; Reflux

2: triethylamine / methanol / 24 h / 20 °C / Inert atmosphere

3: potassium hydroxide / methanol / 4 h / Inert atmosphere; Reflux

4: methanol / 20 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 - 2 °C / Inert atmosphere

6: thiourea / methanol; dichloromethane / 24 h / 20 °C / Inert atmosphere

With iron; ammonium chloride; triethylamine; thiourea; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/jm200566e