t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

Base Information

Chemical Name:t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate
CAS No.:1333379-27-3
Molecular Formula:C₂₂H₂₈N₂O₆S
Molecular Weight:448.54
Hs Code.:

Synonyms:t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

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Chemical Property of t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

Chemical Property:

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Technology Process of t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

There total 5 articles about t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1352810-27-5
C₁₇H₂₀N₂O₄S

: 1333379-27-3
t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm200566e

Reference yield:

: 1333379-26-2
S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

: 1333379-27-3
t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride / methanol; water / 2 h / Inert atmosphere; Reflux

2: triethylamine / methanol / 24 h / 20 °C / Inert atmosphere

With iron; ammonium chloride; triethylamine; In methanol; water;
DOI:10.1021/jm200566e

Reference yield:

: 350672-95-6
4-fluoro-2-(methoxymethoxy)-1-nitrobenzene

: 1333379-27-3
t-butyl (4-(4-((dimethylcarbamoyl)thio)phenoxy)-2-(methoxymethoxy)phenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2: iron; ammonium chloride / methanol; water / 2 h / Inert atmosphere; Reflux

3: triethylamine / methanol / 24 h / 20 °C / Inert atmosphere

With iron; ammonium chloride; caesium carbonate; triethylamine; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm200566e