S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

Base Information

Chemical Name:S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate
CAS No.:1333379-26-2
Molecular Formula:C₁₇H₁₈N₂O₆S
Molecular Weight:378.406
Hs Code.:

Synonyms:S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

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Chemical Property of S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

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Technology Process of S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

There total 2 articles about S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 350672-95-6
4-fluoro-2-(methoxymethoxy)-1-nitrobenzene

: 13511-99-4
dimethyl-thiocarbamic acid S-(4-phenoxyphenyl) ester

: 1333379-26-2
S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm200566e

Reference yield:

: 446-36-6
5-fluoro-2-nitrophenol

: 1333379-26-2
S-(4-(3-(methoxymethoxy)-4-nitrophenoxy)phenyl) dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Cooling with ice

2: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With sodium hydride; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm200566e