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(E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate

Base Information Edit
  • Chemical Name:(E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate
  • CAS No.:1133966-04-7
  • Molecular Formula:C31H33N3O4S
  • Molecular Weight:543.687
  • Hs Code.:
  • Mol file:1133966-04-7.mol
(E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate

Synonyms:(E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of (E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate Edit
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Technology Process of (E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate

There total 9 articles about (E)-methyl 5-(2-(3-(2-(pyridin-2-yl)vinyl)-1-(tetrahydro-2H-pyran-2-yl)-1H-indazol-6-ylthio)phenoxy)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dichloromethane; N,N-dimethyl-formamide; at 80 ℃; for 16h;
Guidance literature:
Multi-step reaction with 3 steps
1.1: ammonium chloride; iron / ethanol; water / 2 h / 50 °C
2.1: hydrogenchloride; sodium nitrite; acetic acid / water / 0 °C
2.2: 2 h / 0 °C
3.1: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 80 °C
With hydrogenchloride; iron; ammonium chloride; caesium carbonate; acetic acid; sodium nitrite; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
Guidance literature:
Multi-step reaction with 5 steps
1.1: methanesulfonic acid / dichloromethane; tetrahydrofuran / 5 h / 25 °C
2.1: N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 12 h / 100 °C
3.1: ammonium chloride; iron / ethanol; water / 2 h / 50 °C
4.1: hydrogenchloride; sodium nitrite; acetic acid / water / 0 °C
4.2: 2 h / 0 °C
5.1: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 80 °C
With hydrogenchloride; methanesulfonic acid; iron; ammonium chloride; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; sodium nitrite; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
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