6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid

Base Information

• Chemical Name: 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid
• CAS No.: 1443136-24-0
• Molecular Formula: C₂₁H₂₃NO₄
• Molecular Weight: 353.418

Synonyms:6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid

Chemical Property of 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid

Chemical Property:

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Technology Process of 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid

There total 2 articles about 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

1-bromo-butane (109-65-9) + 5α-acetoxy-1-methyl-9,10-methylenedioxy-lycoran-4(12)-en-7-one (17431-31-1) → 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid (1443136-24-0)

Guidance literature:

1-bromo-butane; 5α-acetoxy-1-methyl-9,10-methylenedioxy-lycoran-4(12)-en-7-one; In acetonitrile; for 24h; Reflux;

With potassium tert-butylate; In tert-butyl alcohol; for 4h; Reflux;

DOI:10.1016/j.ejmech.2013.03.018

Reference yield:

hippeastrine (477-17-8,30803-79-3) → 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid (1443136-24-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine / 3 h

2.1: acetonitrile / 24 h / Reflux

2.2: 4 h / Reflux

With pyridine; In acetonitrile;

DOI:10.1016/j.ejmech.2013.03.018

Reference yield: 79.0%

methanol (67-56-1) + 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylic acid (1443136-24-0) → methyl 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylate (1443136-34-2)

Guidance literature:

With diazomethyl-trimethyl-silane; In diethyl ether; dichloromethane; at 24 ℃;

DOI:10.1016/j.ejmech.2013.03.018

upstream raw materials:

hippeastrine

1-bromo-butane

5α-acetoxy-1-methyl-9,10-methylenedioxy-lycoran-4(12)-en-7-one

Downstream raw materials:

methyl 6-[2-(butylmethylamino)-3-vinylphenyl]-1,3-benzodioxole-5-carboxylate

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