trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

Base Information

• Chemical Name: trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum
• CAS No.: 1083165-48-3
• Molecular Formula: C₂₃H₂₅Cl₂N₃O₅Pt
• Molecular Weight: 689.455

Synonyms:trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

Chemical Property of trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

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Technology Process of trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

There total 2 articles about trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

trans-bis(benzonitrile)dichloroplatinum(II) (14873-63-3,15617-19-3,51921-56-3) + C-(ethoxycarbonyl)(ethoxycarbonylmethyl)-N-methyl-nitrone (1083165-45-0) → trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum (1083165-48-3)

Guidance literature:

In chloroform; soln. of Pt complex and nitrone (1 equiv.) in CHCl3 was stirred at room temp. for 24-72 h; evapd.; chromd. (SiO2, CH2Cl2/EtOAc, 98/2); elem. anal.;

DOI:10.1039/b807410k

Reference yield:

benzonitrile (100-47-0) → trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum (1083165-48-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzonitrile

2: chloroform

In chloroform; benzonitrile;

DOI:10.1039/b807410k

Reference yield: 82.0%

pyridine (110-86-1) + trans-(benzonitrile)-dichloro[2,3-dihydro-3-ethoxycarbonyl-3-ethoxycarbonyl-methyl-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum (1083165-48-3) → dichloro-bis(pyridine)-platinum(II) (14024-97-6,15227-42-6,14872-21-0)

Guidance literature:

In chloroform; soln. of ligand (5 equiv.) and Pt complex in CHCl3 was heated at 60°C for 24 h;

DOI:10.1039/b807410k

upstream raw materials:

trans-bis(benzonitrile)dichloroplatinum(II)

C-(ethoxycarbonyl)(ethoxycarbonylmethyl)-N-methyl-nitrone

benzonitrile

Downstream raw materials:

trans-[PtCl₂(pyridine)(N=C(Ph)ON(Me)C(CO₂Et)(CH₂CO₂Et))]

dichloro-bis(pyridine)-platinum(II)

trans-[PtCl₂(1-benzyl-2-methylimidazole)(N=C(Ph)ON(Me)C(CO₂Et)(CH₂CO₂Et))]

C₁₆H₂₀N₂O₅

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