Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

Base Information

Chemical Name:Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester
CAS No.:404961-35-9
Molecular Formula:C₁₇H₂₃NO₆
Molecular Weight:337.373
Hs Code.:

Synonyms:Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

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Technology Process of Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

There total 9 articles about Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 13871-68-6
p-aminophenyl acetate

: 1,2:5,6-dianhydro-3,4-O-isopropylidene-D-mannitol

: 404961-35-9
Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

Guidance literature:: In water; at 95 ℃;
DOI:10.1016/S0960-894X(01)00719-3

Reference yield:

: 3969-84-4
3,4-di-O-isopropylidene-D-mannitol

: 404961-35-9
Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 4 h / 0 °C

2: K₂CO₃ / methanol / 2.5 h / 25 °C

3: H₂O / 95 °C

With pyridine; potassium carbonate; In methanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2005.11.090

Reference yield:

: 3969-59-3
mannitol triacetonide

: 404961-35-9
Acetic acid 4-((3aR,4R,8R,8aR)-4,8-dihydroxy-2,2-dimethyl-hexahydro-1,3-dioxa-6-aza-azulen-6-yl)-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. AcOH

2: pyridine / CH₂Cl₂ / 4 h / 0 °C

3: K₂CO₃ / methanol / 2.5 h / 25 °C

4: H₂O / 95 °C

With pyridine; potassium carbonate; acetic acid; In methanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2005.11.090