5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole
CAS No.:917878-56-9
Molecular Formula:C₁₇H₁₆N₆O₂S₃
Molecular Weight:432.551
Hs Code.:

Synonyms:5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

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Chemical Property of 5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

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Technology Process of 5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

There total 6 articles about 5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 917878-64-9
5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylsulfanyl)-1-phenyl-1H-tetrazole

: 917878-56-9
5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2006.09.064

Reference yield:

: 133047-44-6
2-isopropyl-thiazole-4-carboxylic acid ethyl ester

: 917878-56-9
5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 6 steps

1: NH₃ / methanol / 72 h / 20 °C

2: 12.53 g / phosphorus pentasulfide / benzene / 2 h / Heating

3: 94 percent / ethanol / 1 h / Heating

4: 91 percent / LiBH₄ / tetrahydrofuran / 2 h / 20 °C

5: 96 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C

6: 91 percent / aq. H₂O₂; Mo₇O₂₄(NH₄)6*4H₂O / ethanol / 1 h / 20 °C

With diphosphorus pentasulfide; lithium borohydride; ammonium molybdate tetrahydrate; ammonia; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; benzene;
DOI:10.1016/j.tet.2006.09.064

Reference yield:

: 416858-68-9
2-isopropylthiazole-4-carbothioic acid amide

: 917878-56-9
5-(2'-isopropyl[2,4']bithiazolyl-4-ylmethylnesulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / ethanol / 1 h / Heating

2: 91 percent / LiBH₄ / tetrahydrofuran / 2 h / 20 °C

3: 96 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C

4: 91 percent / aq. H₂O₂; Mo₇O₂₄(NH₄)6*4H₂O / ethanol / 1 h / 20 °C

With lithium borohydride; ammonium molybdate tetrahydrate; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tet.2006.09.064