[tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]

Base Information

• Chemical Name: [tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]
• CAS No.: 1159806-88-8
• Molecular Formula: C₄H₁₂N*C₁₈H₄₀N₅NiO₃Si
• Molecular Weight: 535.469
• Mol file: 1159806-88-8.mol

Synonyms:[tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]

Chemical Property of [tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]

There total 1 articles about [tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

K[Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA (1159806-68-4) + tetramethyl ammonium acetate (10581-12-1) + potassium hexamethylsilazane (40949-94-8) → [Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(oxo)](2-) + [tetramethylammonium][Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe3)] (1159806-88-8) + potassium acetate (127-08-2)

Guidance literature:

In N,N-dimethyl acetamide; (Ar); treatment of soln. of nickel compd. in dimethylacetamide with 1 equiv. of potassium amide deriv. at room temp., stirring for 30 min, addn.of tetramethylammonium salt at room temp., stirring for 1 h; filtration, evapn., triturating with diethyl ether, isolation of ppt., recrystn. by diffusion of 1:1 diethyl ether/pentane vapour into soln. in dimethylacetamide, IR and UV;

DOI:10.1039/b820209e

upstream raw materials:

K[Ni(bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

tetramethyl ammonium acetate

potassium hexamethylsilazane