2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Base Information

• Chemical Name: 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin
• CAS No.: 63511-61-5
• Molecular Formula: C₆₀H₆₂N₄
• Molecular Weight: 839.179
• Mol file: 63511-61-5.mol

Synonyms:2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Chemical Property of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

There total 16 articles about 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenyl-porphyrinogen (63456-08-6) → 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin (63511-61-5)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.5h; Heating;

DOI:10.1021/ja00180a029

Reference yield:

acetic acid (64-19-7,77671-22-8) + C60H60N4(2-)*Zn(2+) → zinc diacetate (557-34-6) + 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin (63511-61-5)

Guidance literature:

In dimethyl sulfoxide; at 24.84 - 44.84 ℃; Further Variations:; Solvents; Temperatures; Kinetics;

DOI:10.1134/S1070363208050277

Reference yield:

3,4-diethyl-1H-pyrrole (16200-52-5) + benzaldehyde (100-52-7) → 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin (63511-61-5) + 5,15,10,20-tetraphenylporphyrin (917-23-7,20998-75-8) + (1Z,4Z,9Z,15Z)-2,3-Diethyl-5,10,15,20-tetraphenyl-porphyrin + (1Z,4Z,9Z,15Z)-2,3,7,8-Tetraethyl-5,10,15,20-tetraphenyl-porphyrin

Guidance literature:

With pyrrole; boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) CH₂Cl₂, 2 h;

DOI:10.1016/0040-4039(95)02405-0

upstream raw materials:

2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenyl-porphyrinogen

3,4-diethyl-1H-pyrrole

benzaldehyde

pyrrole

Downstream raw materials:

(chloro)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)iron(III) complex

Co(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)

[Mn(OETPP)Cl]

copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin