copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Base Information

Chemical Name:copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin
CAS No.:146343-94-4
Molecular Formula:C₆₀H₆₀CuN₄
Molecular Weight:900.709
Hs Code.:

Synonyms:copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

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Chemical Property of copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

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Technology Process of copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

There total 3 articles about copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142-71-2
copper diacetate

: 63511-61-5
2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

: 146343-94-4
copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Guidance literature:: In N,N-dimethyl-formamide; at 24.84 ℃;
DOI:10.1134/S1070363217060123

Reference yield:

: 5,10,15,20-tetraphenyl-2,3,7,8,12,13,17,18-octaethyl-21H,23H-porphyne

: 142-71-2
copper diacetate

: 146343-94-4
copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Guidance literature:: In N,N-dimethyl-formamide; Cu-salt was refluxed with ligand in DMF; chromd. on Al2O3 with chloroform;
DOI:10.1023/A:1025673427341

Reference yield:

: 5,10,15,20-tetraphenyl-2,3,7,8,12,13,17,18-octaethyl-21H,23H-porphyne

: 6046-93-1
copper(II) acetate monohydrate

: 146343-94-4
copper(II) complex of 2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin

Guidance literature:: In N,N-dimethyl-formamide; Cu acetate reacted with porphyrin in boiling DMF; according to A. D. Adler, F. R. Longo, F. Kampas, J. Kim, J. Inorg. Nucl. Chem., 1970, 32, 2443; purified by column chromy. (Al2O3, CHCl3); detd. by TLC;
DOI:10.1007/s11172-007-0112-2