2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

Base Information

Chemical Name:2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate
CAS No.:1202634-22-7
Molecular Formula:C₁₆H₁₇Cl₃N₄O₄
Molecular Weight:435.694
Hs Code.:

Synonyms:2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

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Technology Process of 2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

There total 3 articles about 2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 251658-55-6
3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-amine

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1202634-22-7
2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.3390/molecules21050677

Reference yield:

: 636-99-7
4-nitrophenylhydrazine hydrochloride

: 1202634-22-7
2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / 8 h / 80 °C

2: sodium hydrogencarbonate / tetrahydrofuran / 12 h / 0 °C

With hydrogenchloride; sodium hydrogencarbonate; In tetrahydrofuran; ethanol;
DOI:10.3390/molecules200916604

Reference yield:

: 59997-51-2
trimethylacetylacetonitrile

: 1202634-22-7
2,2,2-trichloroethyl (3-(tert-butyl)-1-(4-nitrophenyl)-1H-pyrazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 80 °C

2: tetrahydrofuran / 0 °C

In tetrahydrofuran; ethanol;
DOI:10.3390/molecules21050677