1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

Base Information

Chemical Name:1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate
CAS No.:103905-44-8
Molecular Formula:BF₄*C₂₁H₃₁N*H
Molecular Weight:385.296
Hs Code.:

Synonyms:1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

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Chemical Property of 1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

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Technology Process of 1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

There total 2 articles about 1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 14104-20-2
silver tetrafluoroborate

: di-μ-chlorobis-[[2-(dimethylamino)methyl]phenyl-C,N]dipalladium(II)

: 928-49-4
hex-3-yne

: 103905-44-8
1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

: 7440-05-3
palladium

Guidance literature:: In nitromethane; 3-hexyne in MeNO2 added under N2 to Pd complex and AgBF4 in dry MeNO2, stirred for 6 days at 25°C; removal of solvent in vac., chromy. (SiO2, ether), recrystn. from ether; elem. anal.;

Reference yield: 20.0%

: [(dimethylbenzylaminato^(1-))Pd(acetonitrile)2](BF₄)

: 928-49-4
hex-3-yne

: {C₆H₄CH₂NH(CH₃)2CCH(BF₄)(CC₂H₅)5}

: 103905-44-8
1,2,3,4-tetraethyl-5-{(dimethylammonio)methyl}naphthalene tetrafluoroborate

Guidance literature:: In chlorobenzene; High Pressure; stainless-steel bomb; stirred, heated to 150°C (24 h); filtered; filtrate evapd. to dryness under reduced pressure; residue chromd. on silica gel;
DOI:10.1021/om00113a006