phenyl phenylmethyl disulfide

Base Information

• Chemical Name: phenyl phenylmethyl disulfide
• CAS No.: 16601-17-5
• Molecular Formula: C₁₃H₁₂S₂
• Molecular Weight: 232.37
• Mol file: 16601-17-5.mol

Synonyms:phenyl phenylmethyl disulfide

Chemical Property of phenyl phenylmethyl disulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl phenylmethyl disulfide

There total 47 articles about phenyl phenylmethyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4'-nitrobenzenesulfenanilide (64168-52-1) + phenylmethanethiol (100-53-8) → phenyl phenylmethyl disulfide (16601-17-5)

Guidance literature:

With potassium carbonate; boron trifluoride diethyl etherate; In dichloromethane; for 0.0333333h; Ambient temperature;

DOI:10.1016/S0040-4039(00)84361-0

Reference yield: 89.0%

2-(benzylsulfinothioyl)isoindoline-1,3-dione (33704-38-0) + phenylboronic acid (98-80-6) → phenyl phenylmethyl disulfide (16601-17-5)

Guidance literature:

With [2,2]bipyridinyl; potassium phosphate; copper diacetate; In tetrahydrofuran; water; at 40 ℃; for 10h; Reagent/catalyst; Solvent; Inert atmosphere;

DOI:10.1021/acscatal.9b04326

Reference yield: 88.0%

acetyl benzyl disulfide (5797-02-4) + phenylboronic acid (98-80-6) → phenyl phenylmethyl disulfide (16601-17-5)

Guidance literature:

With [2,2]bipyridinyl; ferrous(II) sulfate heptahydrate; copper(ll) sulfate pentahydrate; trifluorormethanesulfonic acid; oxygen; sodium carbonate; In ethanol; at 25 ℃; Reagent/catalyst; Temperature; Catalytic behavior;

upstream raw materials:

phenylmethanethiol

benzenesulfenyl chloride

2-(benzylthio)pyridine

diphenyldisulfane

Downstream raw materials:

2-(benzylthio)succinic acid

{[(benzylsulfanyl)methyl]sulfanyl}benzene

Benzyl phenyl sulfide

benzenethiosulfonic acid S-benzyl ester