PMP acetal

Base Information

• Chemical Name: PMP acetal
• CAS No.: 56361-94-5
• Molecular Formula: C₈H₁₀O₃
• Molecular Weight: 154.166
• Mol file: 56361-94-5.mol

Synonyms:PMP acetal

Chemical Property of PMP acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PMP acetal

There total 2 articles about PMP acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → PMP acetal (56361-94-5)

Guidance literature:

In aq. phosphate buffer; at 20 ℃; for 24h; pH=7;

DOI:10.3390/molecules22122205

Reference yield:

4-Methoxybenzyl alcohol (105-13-5) → PMP acetal (56361-94-5)

Guidance literature:

Multi-step reaction with 2 steps

1: oxygen; dihydrogen peroxide / Enzymatic reaction

2: aq. phosphate buffer / 24 h / 20 °C / pH 7

With dihydrogen peroxide; oxygen; In aq. phosphate buffer;

DOI:10.3390/molecules22122205

Reference yield: 94.0%

PMP acetal (56361-94-5) + (-)-(2S,3S,4S,6R)-7-[(tert-butyldiphenylsilyl)oxy]-2,4,6-trimethylheptan-1,3-diol (214218-36-7) → tert-butyl((2R,4S)-4-((4S,5S)-2-(4-methoxyphenyl)-5-ethyl-1,3-dioxan-4-yl)-2-methylpentyloxy)diphenylsilane

Guidance literature:

With camphor-10-sulfonic acid; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.24820/ark.5550190.p010.287

upstream raw materials:

4-Methoxybenzyl alcohol

4-methoxy-benzaldehyde

Downstream raw materials:

protonated p-methoxy-benzaldehyde

(E)-2-(4-methoxyphenyl)-5-styryl-1,3-dioxane

1-(4-methoxyphenyl)-N-methylimidazo[1,2-a]quinoxalin-4-amine

4-methoxybenzoic acid