(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

Base Information

Chemical Name:(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene
CAS No.:1338380-91-8
Molecular Formula:C₃₀H₂₇IO₃
Molecular Weight:562.447
Hs Code.:

Synonyms:(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

Chemical Property:

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Technology Process of (3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

There total 4 articles about (3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338380-86-1
C₁₅H₁₅IO₃

: 4801-15-4
3-bromo-1,1-diphenyl-1-propene

: 1338380-91-8
(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1039/c1cc14297f

Reference yield:

: 119-61-9
benzophenone

: 1338380-91-8
(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 7 h / 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -78 - 20 °C

3.1: bromine; triphenylphosphine / dichloromethane / 0.25 h / 0 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With bromine; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc14297f

Reference yield:

: 17792-17-5
ethyl 3,3-diphenylacrylate

: 1338380-91-8
(3-(4-(benzyloxymethyl)-2-iodo-6-methoxyphenoxy)prop-1-ene-1,1-diyl)dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -78 - 20 °C

2: bromine; triphenylphosphine / dichloromethane / 0.25 h / 0 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With bromine; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc14297f